Intermetallic compounds are compounds that, with their high abrasion properties at high temperatures, oxidation resistance in the world today has been widely used. One of the most important of these intermetallic compounds is the aluminide compounds that are used due to the high melting point in industries and equipment such as moweed, which are always used at high temperatures. The Ni-Al, Ti-Al, and Fe-Al compounds are three major categories of these aluminous compounds. Aluminum aluminide compounds are the largest category of aluminides and NiAl compounds. The NiAl composition has properties such as low density (5.9 grams per cubic centimeter), high melting point (1638 degrees centigrade), excellent oxidation resistance, good thermal stability, good electrical conductivity, and high strength to high strength. Among the applied methods of NiAl coatings, it is possible to refer to a variety of thermal spraying processes, membrane coatings, and lamination processes. Variable parameters in this operation are the time and temperature of the heat treatment, the various nickel and aluminum compounds and the parameters affecting the coating for thermal spraying. By carrying out heat treatment at different temperatures and times due to the presence of the penetration phenomenon, the transfer of different elements from the substrate to the coating. Elemental influences seem to alter the structure and phases in the coating, which will affect the wear behavior. By examining the wear behavior of these coatings by wear standard test, the effect of coating parameters and thermal treatment of these coatings on these properties is investigated. The intrusion of the particles of the coating particles into each other during the heat treatment in the vacuum creates interconnecting interactions between the particles, which also increases the coherence of the coating particles. Increasing the amount of oxides during coating heat treatment reduces coherence of coating particles. Increasing the surface roughness of the coating, reducing the oxide layers of Ni and Al elements through thermal treatment are the main factors in increasing the friction coefficient relative to the untreated heat treatment. The heat treatment modifies the wearing mechanisms from the adhesive to the scratching mechanism. This is also the result of an increase in the fraction of intermetallic compounds in the overall coating due to heat treatment, as this phenomenon makes the hardness of the particles separated from the coating (abrasion products) worse during wear. Abrasion products act as micro-abrasives and cause this change of mechanism. The EDS results of the abrasion pattern in all tests show that under different conditions, the coating is not lost due to wear. The increase of intermetallic compounds with favorable mechanical and tribological properties due to heat treatment has reduced the wear rate. Therefore, it can be said that the thermal resistance of the wear resistance increases the coating. It can also be said that the abrasion of the coating at higher temperatures is better because the abrasion rate at 700 ° C has dropped from 400 ° C to 550 ° C.