Zeolites are crystalline, hydrate and nano-porous aluminosilicate materials. These valuable materials are commonly used as commercial adsorbents , and because of their unique structural, physical and chemical properties have many industrial, agricultural, and environmental applications. Zeolites are extensivelyutilized in industry for water purification, for the preparation of advanced materials, for catalytic reactions in petroleum refining, and in nuclear reprocessing. In addition, they are used to separate nitrogen from air to increase oxygen content for both industrial and medical purposes. Currently, theyare usedin large quantities in the production of laundry detergents. The adsorption capacity of zeolites originates from the existence of a porous structure and a net negative charge in their framework, which can lead to attraction and holding of cations. Using zeolites in form of fine powders in purification processes have been limited because of its operational difficulties and the solid-liquid separation stage subsequent to the purification process and. Combining magnetite materials with zeolites and separating them using an external magnetic field, is one of the solutions that has been proposed in the last few years in order to solve or mitigate these problems. In this project, magnetite nano-sorbent was produced from the combination of zeolite-magnetite iron oxide using a process based on vapor phase traort (VPT) method, and its sorption capacity for removal of lead, nickel and chromium ions was investigated. Sorbent synthesis was done in four stages. At first, synthesis of magnetite iron oxide nanoparticles was carried out using co-precipitation method in presence of air using ultra-sonic agitator. Second step was synthesis of NaA zeolite. In order to reduce the size of the zeolite particles and increase the size of its pores, synthesis was performed using microemulsion-ultrasound method. The third step involved the deposition of magnetite particles that were prepared in the first stage using SiO 2 solution. At the final stage, the zeolite particles were used as a coating layer with high absorption capacity for the particles that obtained from the third stage.Finally, the VPT method was used for stabilization of the zeolite layer. In order to evaluate the performance of the obtained sorbent, adsorption of the Pb(II), Ni(II) and Cr(VI) ions from 100mg/l solution of each of this ions were investigated. Also, effect of various parameters such as pH, initial amount of adsorbent and initial concentration of solution on performance of the sorbent was studied. By comparing the result of adsorption test with Freundlich and Langmuir adsorption isotherm models, a good agreement between the experimental data with the Langmuir adsorption isotherm was observed. The maximum value of adsorption for lead, nickel and chromium ions was 232.58, 128.21 and 50.50 milligrams per grams of sorbent, respectively. The adsorbent characteristics were investigated using X-Ray Diffraction (XRD), Scanning Electron microscopy SEM, Fourier Transform Infra-Red (FT-IR), and Vibrating SampleMagnetometer (VSM)instrumental tests, and flame atomic absorption test was used for investigating the remaining concentrations of ions after adsorption. Keywords Magnetite nano-sorbent, magnetite, zeolite, VPT method, heavy metals, adsorptio