Ionic liquids (ILs) have been accepted as very important new green chemicals which have excited both the academia and the chemical industries. This new chemical group can reduce the use of hazardous and polluting organic solvents due to their unique characteristics as well as taking part in various new syntheses. By choosing the correct ionic liquid, high product yields can be obtained, and a reduced amount of waste can be produced in a given reaction. Often the ionic liquid can be recycled, and this leads to a reduction of the costs of the processes. One of the new applications of ionic liquids is in the synthesis of organic compounds including amides. carboxamide ligands have been part of the growing research in the field of coordination chemistry of transition metal complexes. Metal complexes of a wide variety of pyridylamide-based ligands have been studied as structural and/or functional models of several metalloproteins, the binding of metal ions by proteins and peptides if of fundamental interest due to the importance of metal ions in biological systems.Peptides and proteins are able to form coordination complexes with nickel(II) and copper(II) through ligation of deprotonated amide nitrogens. The N-(8-quinolyl)pyridine-2-crboxamide) with the general formula of [M(bpq)X] (M = Cu(II), X = SCN ( 1 ), N 3 ( 2 ); M = Ni(II), X = SCN ( 3 ), N 3 ( 4 )) have been synthesized. In addition the Cu(II) complex of the dianionic ligand bqbza 2- has been prepared. (1) [Cu(bpq)SCN] (2) [Cu(bpq)N 3 ] (3) [Ni(bpq)SCN] (4) [Ni(bpq)N 3 ] (5) [Cu(bqbza)] These complexes have been characterized by UV-Vis, FT-IR, 1 HNMR and elemental analysis. H 2 bqbza ligand and complexes 1 and 5 have been structurally characterized by X-Ray Diffraction . In the structure of H 2 bqbza ligand the benzene ring is nearly coplanar with one of the quinoline ring systems. And the two quinoline ring systems are twisted with respect to each other by a dihedral angle of 74.63.