The current economy is dependent on fossil fuels, which have been seriously challenged by factors such as the growth in demand for oil, which leads to the depletion of non-renewable resources and the political dependence of oil-producing countries. The need to use alternative energy sources has led to the use of clean energies at a much higher level than at present. This justification is sufficient to increase investment in the exploration and exploitation of renewable resources around the world. High power demand requires high performance of rechargeable batteries. For this reason, human beings have begun to build rechargeable batteries. Since the anode plays a very important role in the overall performance of the battery, the anode of lithium ion batteries must have features such as low cost, high electrical conductivity, high energy density and long life cycle. Therefore, electrified nanofibers have been applied to the anode of lithium ion batteries due to their unique properties such as very high surface area to volume ratio, good flexibility, high porosity, thin film created and very low weight. . Today, anode materials are largely carbon-dependent, due to desirable characteristics such as excellent electronic conductivity, lithium ion mobility, availability and low cost. Activated carbon is obtained from pyrolysis of carbon material without the presence of air and its use as anode material due to its high adsorption capacity, high surface area and high porosity as well as low cost compared to other materials make it a unique material. Library studies have so far reported no production of graphene containing polyacrylonitrile nanofibers for precursor production of activated carbon nanofibers containing these particles. Given the specific properties of activated carbon nanofibers and their specific morphology, it can be concluded that the production and investigation of activated carbon nanofibers containing graphene nanoparticles can be of great importance. Polyacrylonitrile solution (10%) was prepared in dimethylformamide and graphene solvents with different percentages (compared to polyacrylonitrile) and electrified at 3 different feed rates and only 4 samples of nanofibers resulted in lower mean diameter and thus Higher specific levels were used to continue the research and perform activation. After activation, all four samples retained their nano-fiber form. FESEM images of polyacrylonitrile nanofibers and BET results showed that after activation of activated carbon nanofibers they showed high surface area and high porosity. By examining the X-ray diffraction patterns of the samples, no significant changes were observed in the crystallinity of polyacrylonitrile nanofibers containing graphene particles after activation. Comparison of FTIR spectra of graphene-containing polyacrylonitrile nanofibers did not show a new reaction or interaction in the nanofibers under the influence of activation on the activated carbon nanofibers containing the said particles. The results of this study can be used in the manufacture of anode lithium ion batteries.