In this study, Accumulative Roll Boning (ARB) and anodizing processes were used as useful proceeses to fabricate the nano Al/Al 2 O 3 /TiC hybrid composite with highly uniform distributed reinforcement particles. By anodizing the aluminum strips at different times, alumina layer with various thicknesses was achieved. Using the anodized strips with different thicknesses of alumina layer and adding TiC particles, Al/Al 2 O 3 /TiC hybrid composites were fabricated with different volume fractions of alumina and TiC particles. Before the fabricating hybrid composite, the peeling test was utilized for evaluating the effective parameters on bond strength of aluminum/aluminum layers. The results of this test demonstrated that increasing the thickness of alumina layer causes to enhance the bond strength of Al/Al layers and by increasing the volume fraction of TiC particles, the bond strength is declined. Microstructur e of composites in different cycles of ARB process was evaluated by scanning electron microscopy (SEM). The microscopic observations showed that after one cycle, departing and fracturing phenomena occurs in brittle alumina layer and by increasing the number of rolling cycles; the alumina fragments break down to finer particles. By applying eight rolling cycles, the distribution of reinforcement particles (Al 2 O 3 and TiC) in aluminum matrix became completely uniform. For evaluating the mechanical properties of produced hybrid composite in different cycles of process, the tensile test, shear punch test and microhardness test were utilized. It was found that if the number of ARB cycles is increased; the mechanical properties of the hybrid composite such as tensile strength, ultimate shear strength and microhardness were enhanced consequently. Elongation of composite samples; decreased dramatically in the first and two steps of composite production (initial four cycles) and it improved by progressing the process to 8th cycle. The results showed that for composites produced by ARB process, the presence of up to 1.6 vol.% alumina and 1 vol.% of TiC particles in aluminum matrix considerably enhance the tensile strength of hybrid composite. Whereas, increasing the amount of alumina and TiC particles more than the said volume fractions, declines the tensile and shear strength. SEM observations of fracture surfaces after tensile test revealed that the failure mode in produced composites by ARB process was shear ductile rupture. The crystallites size that measured by MAUD software for aluminum and the composite produced by eight cycles of ARB process reached to 155 nm and 75 nm, respectively. Finally Al/Al 2 O 3 /TiC hybrid composite was produced by Cross Roll Accumulative Roll bonding (CR-ARB) process. Comparsion of microstructure of ARB and CR-ARB processed composites indicated that the distribution of particles in CR-ARB processed composite is more uniform than the ARB processed composite. The results of investigation of mechanical properties showed that the CR-ARB processed composites have better mechanical properties as tensile and ultimate shear strength, microhardness and elongation. Keywords : Hybrid composites, Al/Al 2 O 3 /TiC, Accumulative roll bonding (ARB), Cros