Zeolite are Aluminasilicate porous material which used chiefly as catalytic, ion exchange and molecular sieve agents to achieve numerous purposes in chemical and petrochemical industries. Over recent years, synthesis of zeolites in nano-scale attracted researchers due to their improved properties. Short crystallization time, lower energy consumption and more conversion percent conducted decrease in production cost. so knowledge about the kinetic of zeolite’s crystallization is very important factor todesign the crystallizer and optimize production process. Two important kinetic’s parameters which impact on crystal size and time of crystallization are nucleation and crystal growth rates. Increasing the nucleation rate perform decreasing crystal size and faster crystallization but enlarge crystal growth rate increase crystal size and crystallization rate. Population balance equation connect the crystal size distribution to crystallization parameters. In this study 4A zeolite was synthesized via hydrogel and micro-emulsion methods and effect of temperature on crystallization rates and it’s kinetic is investigated. XRD analysis showed A type zeolite synthesis from sodium hydroxide via hydrogel and microemulsion methods was successful. Result showed the maximum crystallization time in hydrogel method is more than microemulsion method also at higher crystallization temperature the crystallization rate is faster in both method. minimum crystallization time is 164 and 260 minutes in microemulsion and hydrogel method at 90 ° C. increase in crystallization temperature caused less amount of zeolite was synthesized at the end of crystallization process through hydrogel method but the crystallization temperature has humble effect on this amount. Image analysis on final sample showed that zeolite crystal size which is synthesized via microemulsion method are smaller than hydrogel method also at higher temperature the average crystal size is larger but the impact of crystallization temperature on hydrogel method is more than microemulsion method. At the end of crystallization the minimum average crystal size is 0.716 micrometer by microemulsion method and 1.75 micrometer by hydrogel method which reported at 70 ° C. At continue nucleation profile and crystal growth rate calculated after fitting simulation data to experimental results and effect of crystallization temperature on kinetic’s parameters was investigated then Arrhenius equation used for understanding crystal growth rate relation with crystallization temperature. The results showed at higher temperatures, crystal growth occurred faster also mean crystal growth rate is more in hydrogel method. High value of activation crystal growth energy confirm this reality that reaction on zeolite surface control the growth of zeolite’s crystal also the activation crystal growth energy in microemulsion method is lower than hydrogel method. The nucleation rate profile showed that the average nucleation rate is larger in microemulsion method. Surfactant which parcipitated in microemulsion caused lower interfacial tension in nano-reactor which made from microemulsion and consequently caused increase in nucleation rate by heterogeneous nucleation. Keywords : Zeolite, Crystallization, Nucleation rate, Crystal growth rate, Microemulsion