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SUPERVISOR
Ali-Akbar Ghareh aghaji,Ali Zadhosh
علی اکبر قره آقاجی (استاد راهنما) علی زادهوش (استاد راهنما)
 
STUDENT
Ramazan Abuzade
رمضانعلی ابوزاده گتابی

FACULTY - DEPARTMENT

دانشکده مهندسی نساجی
DEGREE
Doctor of Philosophy (PhD)
YEAR
1385

TITLE

Study of Pores Effect on the Air Permeability of Nanoweb in Theory and Experiment
The nanofibrous structures have received considerable attention in recent years. Because of the extraordinary features such as high porosity, high specific area and desirable functionality; these structures are used in various applications such as filtration and separation, advanced materials, catalysts, drug delivery and tissue engineering, etc... . Suitability of nanofibrous structure for any particular application is highly dependent on its structural characteristics such as porosity. In a nanofibrous structure, nanofiber morphology, pores formed between the nanofibers and the structure permeability are the most important variables that determine its performance. In this study, the air permeability of electrospun poly acrylonitrile nanoweb was evaluated both by theory and experiment considering the pores formed between nanofibers. To achieve this, poly acrylonitrile nanofibers were electrospun in different process and solution conditions. Collecting electrospun nanofibers on paper frame and aluminum foil provide proper samples for air permeability test and scanning electron microscope respectively. By processing the images obtained from scanning electron microscope, the nanofibrous layer structure specifications including nanofiber diameter and nanofiber diameter distribution, number of pores formed between nanofibers, pores area, and pores size distribution were determined. The effect of polymeric solution and electrospinning process variables on the nanofibrous web, structural specifications and air permeability were assessed for further understanding of the relationship between structure geometry and permeability. In the theoretical section, two geometrical models based on geometric probability and Poisson process in two-dimensional space were presented to evaluate the size of the pores formed between the nanofibers. Prediction of both models for the mean radius of pores formed between the nanofibers were compared with the results of image processing and the results of porosimetery. Finally, separate statistical models were presented to predict the air permeability of nanoweb using the data extracted from image processing and also using the electrospinning process data. Both models can explain well the air permeability of nanoweb in the range of mentioned variables. The importance of first model is it ability to determine the air permeability of nanofibrous web using the data from SEM image processing with no need to do air permeability test which is difficult and complex for tiny nanofibrous web samples. The importance of second model is its ability to produce nanofibrous web with certain air permeability.
ساختارهای نانولیفی بخاطر ویژگی های خارق العاده ای که دارند مورد توجه هستند. قابلیت گذردهی یکی از مهمترین خواص سازه های نانولیفی است که عملکرد سازه را در بسیاری از کاربردها مشخص می کند. در این رساله قابلیت گذردهی هوای لایه نانوالیاف پلی اکریلونیتریل الکتروریسی شده مورد مطالعه نظری و تجربی قرار گرفته است. به کمک پردازش تصاویر بدست آمده از میکروسکوپ الکترونی روبشی، مشخصات ساختاری لایه های نانوالیاف شامل قطر و توزیع اندازه قطر نانوالیاف، تعداد منافذ، سطح کلی منافذ و توزیع اندازه منافذ تعیین گردید. در ادامه تاثیر عوامل محلول و فرایند بر مشخصات ساختاری لایه های نانوالیاف و همچنین میزان عبوردهی هوای آنها ارزیابی شد. در بخش مطالعه نظری نیز دو مدل هندسی بر پایه احتمال هندسی و فرایند پواسون ارائه و تحلیل شد. نهایتاً مدل های آماری مجزایی نیز برای پیش بینی میزان عبوردهی هوا از روی ویژگی های ساختاری لایه نانوالیاف مستخرج از پردازش تصویر و همچنین از روی مشخصات فرایند الکتروریسی ارائه شد.

ارتقاء امنیت وب با وف بومی